Preparation and testing of phosphate, oxalate and uric acid matrix-matched standards for accurate quantification of 2D elemental distribution in kidney stone sections using 213 nm nanosecond laser ablation inductively coupled plasma mass spectrometry

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Authors

VAŠINOVÁ GALIOVÁ Michaela ŠTĚPÁNKOVÁ Kateřina ČOPJAKOVÁ Renata KUTA Jan PROKEŠ Lubomír KYNICKÝ Jindřich KANICKÝ Viktor

Year of publication 2015
Type Article in Periodical
Magazine / Source Journal of Analytical Atomic Spectrometry
MU Faculty or unit

Faculty of Science

Citation
Web http://pubs.rsc.org/en/Content/ArticleLanding/2015/JA/C4JA00347K#!divAbstract
Doi http://dx.doi.org/10.1039/c4ja00347k
Field Analytic chemistry
Keywords kidney stones; quantification; matrix-matched calibration standards; LA-ICP-MS
Description Matrix-matched calibration for quantitative elemental mapping of kidney stones by laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS) was developed with a 213 nm Nd:YAG laser ablation device and a quadrupole mass spectrometer. The method was applied to the imaging of P, Na, Sr, Zn, Ba and Pb distributions over a section of the kidney stone specimen containing phosphate and oxalate phases.
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